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学者姓名：卢贝丽
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Abstract ：
本发明公开了一种全生物基胶黏剂及其制备方法和应用，特别适用于木制品制造行业。该技术解决了传统胶黏剂在生产和应用过程中释放有毒气体的问题，并针对化石资源的日益匮乏提供了替代方案。利用中国丰富的竹木资源，本发明采用天然木质素和纤维素为原料，通过一系列创新步骤转化为高效能胶黏剂。首先，将竹粉或木粉与分散剂和水混合，实现原料的充分溶胀和松散；其次，通过机械处理如胶体磨或高压均质机，实现原料的微纳化，得到光滑膏状体；最后，将此膏状体与改性剂和溶剂混合，在特定条件下进行搅拌反应，制备出胶黏剂。该胶黏剂无需移除分散剂和改性剂，因为它们在热压过程中与木质素反应，形成稳定的化学键，提高粘结效果。
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| GB/T 7714 | 黄彪 , 唐丽荣 , 吕建华 et al. 一种全生物基胶黏剂及其制备方法和应用 : CN202410263383.5[P]. | 2024-03-08 . |
| MLA | 黄彪 et al. "一种全生物基胶黏剂及其制备方法和应用" : CN202410263383.5. | 2024-03-08 . |
| APA | 黄彪 , 唐丽荣 , 吕建华 , 卢贝丽 , 刘瀚杨 , 游昕达 et al. 一种全生物基胶黏剂及其制备方法和应用 : CN202410263383.5. | 2024-03-08 . |
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本发明公开了一种木沥青基多孔碳材料及其制备方法，其是利用木沥青与过氧化氢进行反应制得氧化木沥青，然后将所得氧化木沥青与壳聚糖、丙烯酸松香混合进行预碳化，再将所得产物与KOH混合进行活化，从而制得松香‑木沥青基多孔碳材料。采用直接墨水书写技术（DIW），可将利用本发明所得松香‑木沥青基多孔碳材料为原料制得的复合墨水打印成电极，从而用于全凝胶态微型超级电容器的制备，其所得超级电容器兼具优异的打印性能和电化学活性。
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| GB/T 7714 | 唐丽荣 , 谭宁宁 , 黄彪 et al. 一种木沥青基多孔碳材料的制备及其在3D打印超级电容器中的应用 : CN202410676807.0[P]. | 2024-05-29 . |
| MLA | 唐丽荣 et al. "一种木沥青基多孔碳材料的制备及其在3D打印超级电容器中的应用" : CN202410676807.0. | 2024-05-29 . |
| APA | 唐丽荣 , 谭宁宁 , 黄彪 , 卢贝丽 , 吕建华 , 游昕达 et al. 一种木沥青基多孔碳材料的制备及其在3D打印超级电容器中的应用 : CN202410676807.0. | 2024-05-29 . |
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本发明公开了一种金属氧化物原位负载的颗粒炭催化剂及其制备方法和应用，其是采用木薯淀粉、柠檬酸、含氮化合物和金属盐形成的交联体系作为粘结物质，通过其与生物质原料的相互作用促进交联成型，再经过捏合挤条、整形造粒、固化和高温炭化等工艺，制备得到具有良好机械强度的颗粒炭催化剂，其中所用金属离子不仅有利于加速交联体系的形成，还能够在高温炭化过程中转化为均匀分散的金属氧化物纳米颗粒，原位负载于颗粒炭上，增加颗粒炭催化剂的催化活性位点，使其在松香酯化反应中表现出优异的催化性能。本发明实现了粘结成型与高催化性能的兼顾，所得催化剂还具有低成本和易回收的优势，为环境友好的催化材料的开发提供了新的途径。
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| GB/T 7714 | 卢贝丽 , 左志瑞 , 詹鑫琳 et al. 一种金属氧化物原位负载的颗粒炭催化剂及其制备方法和应用 : CN202510508139.5[P]. | 2025-04-22 . |
| MLA | 卢贝丽 et al. "一种金属氧化物原位负载的颗粒炭催化剂及其制备方法和应用" : CN202510508139.5. | 2025-04-22 . |
| APA | 卢贝丽 , 左志瑞 , 詹鑫琳 , 吴瑞锋 , 黄彪 , 吕建华 et al. 一种金属氧化物原位负载的颗粒炭催化剂及其制备方法和应用 : CN202510508139.5. | 2025-04-22 . |
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本发明涉及一种非对称荷电共价有机框架复合醋酸纤维素纳滤膜及其制备方法和应用。通过将COF纳米片分散于DMF中，再加入丙酮和醋酸纤维素，配制成铸膜液，经过搅拌和脱泡，使用刮涂的方法，再预挥发相应时间，在去离子水中相转化成膜。本发明采用表面偏析技术，将高电荷密度的COF材料在膜内构筑非均匀分布的荷电结构。所得非对称荷电共价有机框架复合醋酸纤维素纳滤膜应用于离子纳滤，性能较好，可实现纳滤脱盐，在海水淡化、废水处理等行业极具前景。
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| GB/T 7714 | 游昕达 , 陈冉 , 宋子凡 et al. 一种非对称荷电共价有机框架复合醋酸纤维素纳滤膜的制备方法和应用 : CN202411564880.5[P]. | 2024-11-05 . |
| MLA | 游昕达 et al. "一种非对称荷电共价有机框架复合醋酸纤维素纳滤膜的制备方法和应用" : CN202411564880.5. | 2024-11-05 . |
| APA | 游昕达 , 陈冉 , 宋子凡 , 罗珊 , 曾睿远 , 刘瀚杨 et al. 一种非对称荷电共价有机框架复合醋酸纤维素纳滤膜的制备方法和应用 : CN202411564880.5. | 2024-11-05 . |
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本发明公开了一种竹木基生物环氧胶黏剂的制备方法及其应用，其是通过将竹/木原料粉碎并磨粉后，将所得粉体与多元醇和水混合并静置，之后通过机械研磨实现竹粉、木粉的微纳化；再将其与环氧化合物、多元酸/酸酐和溶剂混合，经搅拌反应制得所述竹木基生物环氧胶黏剂。本发明利用丰富的竹木资源，创新性地开发了一种全新的胶黏剂，其具有优异的粘接强度、耐水性、耐热性以及良好的环境友好性，可直接应用于通过热压实现固化粘合的领域，如制备胶合板、纤维板、刨花板、竹木复合板等，以应对传统石油基胶黏剂的环境和健康问题，同时克服了现有生物基胶黏剂在粘接性能方面的不足。
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| GB/T 7714 | 黄彪 , 刘瀚杨 , 唐丽荣 et al. 一种竹木基生物环氧胶黏剂的制备方法和应用 : CN202410265523.2[P]. | 2024-03-08 . |
| MLA | 黄彪 et al. "一种竹木基生物环氧胶黏剂的制备方法和应用" : CN202410265523.2. | 2024-03-08 . |
| APA | 黄彪 , 刘瀚杨 , 唐丽荣 , 卢贝丽 , 吕建华 , 游昕达 et al. 一种竹木基生物环氧胶黏剂的制备方法和应用 : CN202410265523.2. | 2024-03-08 . |
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本发明公开了一种环氧大豆油‑木质素‑多元酸三元胶黏剂及其制备方法和应用，其是将木质素、多元醇和水混合后进行机械研磨，然后将研磨产物与环氧大豆油、多元酸/酸酐和溶剂混合搅拌或研磨，从而得到所述三元胶黏剂。本发明充分利用了木质素和环氧大豆油的天然优势，通过简化的制备方法，提高了胶黏剂的整体性能，解决了传统石油基胶黏剂存在有害物质释放，而生物基胶黏剂在高湿度或高温环境下性能稳定性受限的问题。该胶黏剂可广泛应用于胶合板、纤维板、刨花板、竹木复合板等领域，具有优异的环保性能和工业应用性能。
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| GB/T 7714 | 刘瀚杨 , 黄彪 , 卢贝丽 et al. 一种环氧大豆油-木质素-多元酸三元胶黏剂及制备方法 : CN202410265557.1[P]. | 2024-03-08 . |
| MLA | 刘瀚杨 et al. "一种环氧大豆油-木质素-多元酸三元胶黏剂及制备方法" : CN202410265557.1. | 2024-03-08 . |
| APA | 刘瀚杨 , 黄彪 , 卢贝丽 , 唐丽荣 , 吕建华 , 游昕达 et al. 一种环氧大豆油-木质素-多元酸三元胶黏剂及制备方法 : CN202410265557.1. | 2024-03-08 . |
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Sensing materials derived from natural and biodegradable sources are increasingly being developed and applied to realize environmentally friendly technologies. In this paper, we present the synthesis, characterization, and application of a novel copper abietate/polyvinyl acetate (CuA/PVAc) composite film, specifically engineered to enhance the humidity-sensing capabilities of Chinese herbal medicine monitoring systems. The sensing material was synthesized by strategically melding copper abietate, a natural renewable material, with PVAc to exploit their combined synergistic properties for optimal humidity-sensing performance. Comprehensive characterization techniques, including inductively coupled plasma optical emission spectrometry (ICP-OES), field-emission scanning electron microscopy (FESEM), water contact angle measurements, and Fourier transform infrared (FT-IR) spectroscopy, were employed to confirm the formation of CuA/PVAc composites. These analyses confirmed the homogeneity and intended chemical composition of the composite films.The resultant CuA-1/PVAc-4 (0.4 mu g/mu L) composite film exhibited a good logarithmic relation (0.9988) with relative humidity (RH) over a wide range (11 %-97 %) and high sensitivity (24.55 Hz/%RH). Moreover, this study introduces a novel, eco-friendly approach by integrating the CuA/PVAc composite with a quartz crystal microbalance (QCM) sensor and a sophisticated wireless circuit that enables real-time, Wi-Fi-based humidity monitoring tailored for the preservation of Chinese herbal medicines. The implementation of this wireless humidity detection system represents a significant advancement in the application of environmentally friendly materials in sensor technology and offers a practical and scalable approach for precise environmental monitoring.
Keyword ：
Chinese herbal medicine Chinese herbal medicine Copper abietate/Polyvinyl acetate Copper abietate/Polyvinyl acetate Humidity sensing Humidity sensing Renewable Renewable Wireless environmental monitoring Wireless environmental monitoring
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| GB/T 7714 | Tan, Ningning , Weng, Yaohang , Li, Haijun et al. Copper abietate/polyvinyl acetate composite film for enhanced humidity sensing in Chinese herbal medicine monitoring systems [J]. | SENSORS AND ACTUATORS B-CHEMICAL , 2025 , 422 . |
| MLA | Tan, Ningning et al. "Copper abietate/polyvinyl acetate composite film for enhanced humidity sensing in Chinese herbal medicine monitoring systems" . | SENSORS AND ACTUATORS B-CHEMICAL 422 (2025) . |
| APA | Tan, Ningning , Weng, Yaohang , Li, Haijun , Chen, Bo , Zhao, Lan , Huang, Biao et al. Copper abietate/polyvinyl acetate composite film for enhanced humidity sensing in Chinese herbal medicine monitoring systems . | SENSORS AND ACTUATORS B-CHEMICAL , 2025 , 422 . |
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The development of efficient catalysts for rosin esterification is essential for advancing the high-value utilization of natural rosin, owing to the improvements in its processability. This study focused on the preparation of the magnesium oxide/N-doped biochar (B-MgO-N-C) from wood waste using a mechanochemistry-assisted strategy. Comprehensive characterizations revealed that ball milling together with nitrogen doping facilitated the incorporation of MgO into the carbon matrix, both of which contributed to the improved catalytic activity. The catalytic performance of B-MgO-N-C was then evaluated using the esterification of rosin with glycerol as a model reaction. After optimization, a 94.6 % rosin conversion was achieved at 230 degrees C over 4 h, outperforming the performance of both MgO-loaded biochar and N-doped biochar catalysts. The enhanced catalytic activity of BMgO-N-C can be attributed to the synergistic effect of in-situ embedded MgO and N-doping, which increases the number of active sites. CO2-TPD and NH3-TPD studies confirmed the importance of basic sites in promoting the esterification of rosin, whereas acidic sites might also contribute to this process. Moreover, recycling tests demonstrated that N-doping improved the stability of B-MgO-N-C. The catalyst also showed high rosin conversion when other alcohols were used. Accordingly, this work presents a straightforward strategy for designing metal oxides/N-doped biochar as advantageous catalysts for the esterification of rosin.
Keyword ：
Esterification Esterification Heterogeneous catalysis Heterogeneous catalysis Magnesium oxide Magnesium oxide Mechanochemistry Mechanochemistry N -doped biochar N -doped biochar Rosin Rosin
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| GB/T 7714 | Zuo, Zhirui , Xu, Yunzhuo , Yan, Chenrui et al. Mechanochemistry-assisted synthesis of MgO/N-doped biochar from wood waste for synergistic catalysis in rosin esterification [J]. | INDUSTRIAL CROPS AND PRODUCTS , 2025 , 226 . |
| MLA | Zuo, Zhirui et al. "Mechanochemistry-assisted synthesis of MgO/N-doped biochar from wood waste for synergistic catalysis in rosin esterification" . | INDUSTRIAL CROPS AND PRODUCTS 226 (2025) . |
| APA | Zuo, Zhirui , Xu, Yunzhuo , Yan, Chenrui , Wu, Ruifeng , You, Xinda , Liu, Hanyang et al. Mechanochemistry-assisted synthesis of MgO/N-doped biochar from wood waste for synergistic catalysis in rosin esterification . | INDUSTRIAL CROPS AND PRODUCTS , 2025 , 226 . |
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In this study, a novel proton-conducting film was strategically engineered by interfacial manipulation of green and sustainable biomass resources guanine and phosphorylated cellulose nanocrystals (PCNCs) within vermiculite layers. The interfacial engineering approach involved regulation of molecular interactions at the vermiculite-organic interface, whereby PCNCs were incorporated into the interlayers of guanine/vermiculite composites. This interfacial assembly process guided guanine to form tubular structures or ultrathin nanosheets architectures, enabling the fabrication of guanine/vermiculite-PCNCs (G/VMT-PCNCs) composite films with an active-site-rich and tightly interconnected network via a vacuum-assisted process. The rationally designed composite films exhibited excellent proton conductivity, which showed positive correlation with relative humidity (RH) and temperature, reaching 0.50 mS/cm at 25 degrees C and 97 %. Notably, the optimal composite film achieved a maximum proton conductivity of 1.15 mS/cm at 97 % RH and 80 degrees C. The interface-engineered structure endowed the humidity sensors based on this composite film with superior performance, including high sensitivity (31.82 Hz/%RH), small hysteresis (0.60 % RH), and rapid response/recovery times (36 s/5 s). The findings provide valuable insights into the design and fabrication of high-performance proton exchange films and humidity sensors, contributing to the advancement of sustainable clean energy technologies.
Keyword ：
Biomass-derived materials Biomass-derived materials Confined self-assembly Confined self-assembly Humidity sensor Humidity sensor Phosphorylated cellulose nanocrystals (PCNCs) Phosphorylated cellulose nanocrystals (PCNCs) Proton conductivity Proton conductivity
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| GB/T 7714 | Tang, Lirong , Wu, Junwei , Cao, Zhiyi et al. Interfacial engineered biomass-derived G/VMT-PCNCs networks as high-performance proton-conducting humidity sensors [J]. | CARBOHYDRATE POLYMERS , 2025 , 356 . |
| MLA | Tang, Lirong et al. "Interfacial engineered biomass-derived G/VMT-PCNCs networks as high-performance proton-conducting humidity sensors" . | CARBOHYDRATE POLYMERS 356 (2025) . |
| APA | Tang, Lirong , Wu, Junwei , Cao, Zhiyi , Hong, Qiqi , Lin, Fengcai , Tan, Ningning et al. Interfacial engineered biomass-derived G/VMT-PCNCs networks as high-performance proton-conducting humidity sensors . | CARBOHYDRATE POLYMERS , 2025 , 356 . |
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Tetracycline (TC) and its derivatives pose a serious threat to the ecological environment and human health due to their high toxicity and difficult degradation, and there is an urgent need to develop an effective degradation technology for their efficient removal. In this study, FeP/phosphorus-doped carbon aerogel (FeP/PCA) with dual advantages of degradation and adsorption was constructed by a one-step synthesis strategy using sodium carboxymethyl cellulose (CMC) as a carbon source, phytic acid as a phosphorus source, and ferric chloride as an iron source, and was applied as an advanced oxidation catalyst for the removal of TC. Under the combined effect of adsorption, in situ oxygen activation and electron transfer, FeP/PCA achieved 100 % removal and 72.9 % mineralization of TC. Desorption and Ar pre-blowing experiments showed that the contributions of FeP/PCA to the adsorption, in situ oxygen activation, and electron transfer were 53.2 %, 28.0 %, and 18.8 %, respectively. FeP/PCA adsorbed dissolved oxygen (DO) from water and induced in-situ oxygen activation through FeP and carbon substrate defects, which drove the Fenton-like reaction to generate reactive oxygen species (center dot O2-, center dot OH, and 1 O 2 ) to efficiently degrade TC. Among them, center dot O 2 - provides a primary role. In addition, FeP induced changes in the electronic structure of PCA, leading to electron transfer of sp2 C--C, sp3 C-C, C-O/C-P and C--O, resulting in a synergistic degradation effect. This study presents for the first time a novel composite material with both adsorption and catalytic degradation advantages that can be used for the practical treatment of antibiotic wastewater.
Keyword ：
FeP/PCA FeP/PCA Iron-based catalysts Iron-based catalysts Phosphorus doping Phosphorus doping Reactive oxygen species Reactive oxygen species Tetracycline Tetracycline
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| GB/T 7714 | Wang, Guilong , Jiang, Rongyuan , Chen, Juntao et al. One-step construction of FeP/carbon aerogel composites and their efficient tetracycline removal mechanisms: Adsorption, in situ oxygen activation and electron transfer [J]. | JOURNAL OF WATER PROCESS ENGINEERING , 2025 , 70 . |
| MLA | Wang, Guilong et al. "One-step construction of FeP/carbon aerogel composites and their efficient tetracycline removal mechanisms: Adsorption, in situ oxygen activation and electron transfer" . | JOURNAL OF WATER PROCESS ENGINEERING 70 (2025) . |
| APA | Wang, Guilong , Jiang, Rongyuan , Chen, Juntao , Li, Simin , Lin, Guanfeng , Lu, Beili et al. One-step construction of FeP/carbon aerogel composites and their efficient tetracycline removal mechanisms: Adsorption, in situ oxygen activation and electron transfer . | JOURNAL OF WATER PROCESS ENGINEERING , 2025 , 70 . |
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